Preparation of forsterite refractory using highly abundant amorphous rice husk silica for thermal insulation

Abstract

The aim of the study was to investigate the effect of amorphous silica on the phase formation and study the physical characteristics of forsterite refractory prepared from quartz and MgO powder. Various samples were subjected to sintering temperature around 1100 °C and development of forsterite phase was characterized using Fourier Transform Infrared (FTIR) spectroscopy, X-ray diffraction (XRD), and scanning electron microscopy (SEM). The result indicate that the addition of rice husk ash (RHA) significantly affect the formation of forsterite phase. As the amount of RHA increased, it led to a better reaction between amorphous silica and periclase, later that will transform into forsterite phase at a temperature around 1100 °C. Formation of forsterite resulted in decrease of density, porosity, and thermal conductivity, while the opposite was observed for Cold Crushing Strength. Formation of forsterite phase was identified by XRD analysis of the sample. Based on the characteristics, the samples were considered as an insulator and of the potential use as refractory devices. © 2017 The Ceramic Society of Japan and the Korean Ceramic Society