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Synthesis and characterization of organotin(IV) thiobiurets

dc.contributor.authorRastogi R.B.; Singh K.; Maurya J.L.
dc.date.accessioned2025-05-24T09:15:01Z
dc.description.abstractSome triphenyltin and dibutyltin thiobiurets of the type Ph 3SnL and Bu 2SnL 2/ [where LH = 1,5 diphenyl-2-thiobiuret (PPTBH), 1-(4-ethoxyphenyl)-5-phenyl-2-thiobiuret (EtOPPTBH), or 1-naphthyl-5-phenyl-2-thiobiuret (naphPTBH)], have been synthesized and characterized by elemental analysis and various physicochemical techniques. Molar conductance measurements show the non-ionic behavior of the complexes. FAB mass spectra exhibit their monomeric nature. 1H and 13CNMR spectra support the proposed stoichiometry of the complexes. Infrared spectra suggest monoanionic bidentate mode of bonding of the ligands. The powder XRD patterns of the complex Bu 2Sn (PPTB) 2are indicative of triclinic crystal system. Copyright © Taylor & Francis Group, LLC.
dc.identifier.doihttps://doi.org/10.1080/15533174.2011.614309
dc.identifier.urihttp://172.23.0.11:4000/handle/123456789/13412
dc.relation.ispartofseriesSynthesis and Reactivity in Inorganic, Metal-Organic and Nano-Metal Chemistry
dc.titleSynthesis and characterization of organotin(IV) thiobiurets

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